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Publication:
Comparison of analytical methods used for measuring major ions in the EPICA Dome C (Antarctica) ice core

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dc.contributor.authorLittot, Geneviève C.
dc.contributor.authorMulvaney, Robert
dc.contributor.authorRöthlisberger, Regine
dc.contributor.authorUdisti, Roberto
dc.contributor.authorWolff, Eric W.
dc.contributor.authorCastellano, Emiliano
dc.contributor.authorde Angelis, Martine
dc.contributor.authorHansson, Margareta E.
dc.contributor.authorSommer, Stefan
dc.contributor.authorSteffensen, Jørgen P.
dc.date.accessioned2024-09-02T17:49:48Z
dc.date.available2024-09-02T17:49:48Z
dc.date.issued2002
dc.description.abstractIn the past, ionic analyses of deep ice cores tended to consist of a few widely spaced measurements that indicated general trends in concentration. the ion-chromatographic methods widely used provide well-validated individual data, but are time-consuming. the development of continuous flow analysis (CFA) methods has allowed very rapid, high-resolution data to be collected in the field for a wide range of ions. In the European Project for Ice Coring in Antarctica (EPICA) deep ice-core drilling at Dome C, many ions have been measured at high resolution, and several have been analyzed by more than one method. the full range of ions has been measured in five different laboratories by ion chromatography (IC), at resolutions of 2.5–10 cm. In the field, CFA was used to measure the ions Na+, Ca2+, nitrate and ammonium. Additionally, a new semi-continuous in situ IC method, fast ion chromatography (FIC), was used to analyze sulphate, nitrate and chloride. Some data are now available to 788 m depth. In this paper we compare the data obtained by the three methods, and show that the rapid methods (CFA and FIC) give an excellent indication of trends in ionic data. Differences between the data from the different methods do occur, and in some cases these are genuine, being due to differences in speciation in the methods. We conclude that the best system for most deep ice-core analysis is a rapid system of CFA and FIC, along with in situ meltwater collection for analysis of other ions by IC, but that material should be kept aside for a regular check on analytical quality and for more detailed analysis of some sections.
dc.description.numberOfPages7
dc.identifier.doi10.48350/158768
dc.identifier.publisherDOI10.3189/172756402781817022
dc.identifier.urihttps://boris-portal.unibe.ch/handle/20.500.12422/43376
dc.language.isoen
dc.publisherInternational Glaciological Society
dc.relation.ispartofAnnals of glaciology
dc.relation.issn0260-3055
dc.relation.organizationDCD5A442BF29E17DE0405C82790C4DE2
dc.subject.ddc500 - Science::530 - Physics
dc.titleComparison of analytical methods used for measuring major ions in the EPICA Dome C (Antarctica) ice core
dc.typearticle
dspace.entity.typePublication
oaire.citation.endPage305
oaire.citation.startPage299
oaire.citation.volume35
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unibe.date.licenseChanged2021-09-21 13:20:50
unibe.description.ispublishedpub
unibe.eprints.legacyId158768
unibe.journal.abbrevTitleANN GLACIOL
unibe.refereedTRUE
unibe.subtype.articlejournal

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